Practical Electron Microscopy and Database

An Online Book, Second Edition by Dr. Yougui Liao (2006)

Practical Electron Microscopy and Database - An Online Book

Chapter/Index: Introduction | A | B | C | D | E | F | G | H | I | J | K | L | M | N | O | P | Q | R | S | T | U | V | W | X | Y | Z | Appendix

Cathodoluminescence System and Their Troubleshooting

Examples of cathodoluminescence systems are:
         i) Gatan MonoCL4 cathodoluminescence spectrometer.
         ii) ChromaCL2 iBSED Detector.

Issues can occur in cathodoluminescence systems, for instance:
         i) Missing certain wavelengths of the cathodoluminescence spectrum because:
         i.a) Filters placed in front of the cathodoluminescence spectrometer can eliminate certain luminescence and phosphorescence.
         i.b) Incorrect sample height (focal point) because the spectrometer (e.g. Gatan MonoCL4 cathodoluminescence spectrometer) needs a different geometry for optimizing the collection of certain wavelengths.
         i.c) The gain of longer wavelengths is too weak to detect for photomultiplier-based detectors.
         ii) It breaks microscope vacuum sometimes when it is inserted into the column. Possible reasons are cracks in vacuum bellows, or worn-out O-ring.