Table 3277. History of In Situ/environmental TEM/STEM observations.
Year |
Researcher |
Details |
References |
2001 |
Hansen/Haldor
Topsoe |
With Phillips CM
200 FEG, in resolution of 0.23 nm, under pressure of 4 Torr
H2/N2, and at temperature of /550 °C |
[2,3] |
1994 |
Sharma et al. |
With Phillips 400T, in resolution of 0.42 nm, under pressure of 3 Torr of NH3 |
[5] |
1991 |
Yao, Spindler, Gatan Inc. |
With Phillips CM 30, in resolution of 0.34 nm, under pressure of 20 Torr |
[4] |
1991 |
Doole, Parkinson,
Hutchinson |
With JEOL 4000, in resolution of 0.31 nm, under pressure of 4.2 Torr of
H2, and at temperature of 670 °C |
[6] |
... |
|
Moved very slow because: i) Difficulties on instrumentation; ii)
Difficulties on resolution; iii) Lack of funding |
|
Early to mid 1970 |
D. L. Allison in USA |
Physical sciences |
|
Early 1960 |
H. G. Heide in Germany |
Biological science (gas controlled environment) |
|
Late 1950 to early 1960 |
Stoyanova, I. G., in Russia |
Biological sciences (gas and wet cell), first to examine wet biological materials in TEM |
|
Late 1950 |
T Ito in Japan |
Physical sciences/Instrumentation (gas interaction) |
|
1944 |
Abrams and McBain |
Constructed the first enclosed wet cell |
|
1935 |
L. Marton |
In-Situ TEM/STEM method with a windowed cell: the sample is sandwiched between two electron transparent thin films in order to examine biological materials in hydrated
state (e.g. amorphous carbon films) |
[1] |
[1] L. Marton, Nature 133, 911 (1935).
[2] L. Hansen and J. B. Wagner, Proc. 12th European Congress on Electron Microscopy, Vol. II, (2000) 537–538.
[3] ThomasW. Hansen, Jacob B.Wagner, Poul L. Hansen, Seren Dahl, Haldor Topsoe, Claus J. H. Jacobson,
Science, 294 (2001) 1508–1510.
[4] Nan Yao, Gerard E. Spinnler, Richard A. Kemp, Don C. Guthrie, R. Dwight Cates and C. Mark
Bolinger, Proc. 49th Annual; meeting of Microsc. Soc. Am. San Francisco Press (1991) 1028.
[5] Renu Sharma, K. Weiss, M. McKelvy and W. Glaunsinger, Proc. 52nd Ann. Meet. Microscopy Society of
America, (1994) 494–495P.
[6] R. C. Doole, G.M. Parkinson, J. L. Hutchison, M. J. Goringe and P. J. F. Harris JEOL News 30E,
(1992) 30.
|